1.  Safety
2.
Objectives/Overview
3.
Procedures
4. Observations
5.
Equipment
6.

View Techniques:
Acid-Base Titration
- Preparing Burette
- H2SO4 Solutions
- Titration

7. Sample Calculations
8.

Waste Disposal/Clean-up

9. Calculations/Set-ups
10. Conclusions
11. Grading Scale
12.
Review Prelab Questions
13. Review Postlab Questions

Experiment 5
Standardization of NaOH by Titration

WASTE DISPOSAL

WARNING: Reserve the unused diluted NaOH solution in the Florence flask for the next experiment. Label with your name and Section Number and store as directed.

Notes:

  • Titrated solutions (pink) should be disposed of down the drain followed by tap water.
  • Any remaining waste acid or base solutions should be discarded in the designated Acid-Base Waste container.

CLEAN-UP

WARNING: Reserve the unused diluted NaOH solution in the Florence flask for the next experiment. Label with your Name and Section Number and store as directed.

Notes:

  • Drain the burette and dispose of remaining NaOH from the burette in the designated Acid-Base Waste container.
  • Your pipette should be rinsed well with tap water followed by distilled water.
  • Rinse the burette five times with ten mL portions of distilled water to remove all traces of NaOH from the burette and tip.
  • Leave the burette filled with distilled water and the funnel inverted on the top.
  • A 10 point deduction will be incurred if the instructor detects base in the burette.
  • Wipe your bench-top thoroughly with wet paper towels to remove any traces of acid or base.
  • Assure that no paper towels have been placed in the sinks.
 
 
 
 
 
 

 

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